Study guide

Required Practicals: A Skills Checklist

Lab Techniques & AnalysisBeginner7 min read
On this page
  1. How to use the checklist
  2. 1. Working safely
  3. 2. Measuring mass
  4. 3. Measuring volume
  5. 4. Titration
  6. 5. Making a standard solution
  7. 6. Heating safely
  8. 7. Separating and purifying
  9. 8. Identifying substances
  10. 9. Measuring rates and energy changes
  11. 10. Recording data
  12. 11. Graphs
  13. 12. Evaluating
  14. Turning the checklist into a plan
  15. Key takeaways

Most chemistry courses include a set of required or core practicals, and exam questions about them are common: describe how you would…, explain why…, suggest an improvement… Whatever syllabus you follow, the same underlying skills come up again and again. This checklist lets you rate yourself on each one, shows what a confident answer or technique looks like, and points you to a guide for anything you’re unsure of.

How to use the checklist

For each skill, give yourself a rating:

  • 3 – I can do this confidently and explain why each step matters.
  • 2 – I can do it, but I’m unsure of some details or reasons.
  • 1 – I haven’t done this, or I’d need help.

Focus revision on your 1s and 2s. Come back in a few weeks and re-rate.

1. Working safely

Skill What “good” looks like
Identify hazards from symbols and labels You can name the meaning of each GHS pictogram. See hazard symbols.
Write a simple risk assessment You state the hazard, the risk and a specific control measure (not just “be careful”). See risk assessment.
Choose the right protection Eye protection always; gloves and a fume cupboard when the chemicals require them.
Deal with spills and breakages You know to tell the teacher, and how small spills are neutralised or absorbed.

Exam tip: “Wear goggles” earns credit only when it’s linked to a specific hazard: “wear eye protection because sodium hydroxide is corrosive to eyes.”

2. Measuring mass

Skill What “good” looks like
Use a top-pan balance correctly Tare (zero) with the container on; add solid away from the balance pan; close draughts. See using a balance.
Weigh by difference Weigh the container with solid, transfer, reweigh the container; the difference is the mass transferred.
Record to the balance’s resolution e.g. 2.45 g on a 0.01 g balance, not 2.4 or 2.450.

3. Measuring volume

Skill What “good” looks like
Choose the right equipment Measuring cylinder for approximate volumes; pipette or burette for accurate ones. See measuring volume accurately.
Read a meniscus Eye level, bottom of the meniscus for clear liquids, on a white background.
Use a pipette Rinse with the solution, fill with a pipette filler past the mark, adjust to the mark, drain with the tip touching the flask.
Use a burette Rinse with titrant, fill, remove air bubble from the tip, read to ±0.05 cm³.

See volumetric glassware tolerances for the uncertainties of each item.

4. Titration

Skill What “good” looks like
Carry out rough and accurate titrations A quick rough titre, then accurate titres adding drop by drop near the end point.
Swirl and use a white tile The colour change is seen clearly and the end point is not overshot.
Obtain concordant results Titres within 0.10 cm³ of each other; the mean is calculated from these only.
Choose an indicator Matches the pH range of the steep part of the curve. See choosing an indicator.

Full walk-through: acid–base titration. Common problems: titration errors.

5. Making a standard solution

Skill What “good” looks like
Dissolve the solid fully Weigh, dissolve in a beaker with some distilled water, then transfer.
Transfer without loss Rinse the beaker and glass rod into the volumetric flask several times.
Make up to the mark Add water until the bottom of the meniscus sits on the line, dropwise at the end.
Mix Stopper and invert the flask many times.

6. Heating safely

Skill What “good” looks like
Choose a heat source Water bath or electric heater for flammable liquids; Bunsen for non-flammable solutions.
Heat a test tube Hold at an angle, pointing away from people, heating gently near the surface.
Heat to constant mass Heat, cool, weigh; repeat until two masses agree, showing the reaction is complete. See hydrates.

7. Separating and purifying

Skill What “good” looks like
Filtration Folded filter paper in a funnel, wet to seat it; residue washed with small portions of cold solvent.
Evaporation and crystallisation Heat to concentrate, then let it cool slowly so larger, purer crystals form.
Simple distillation Thermometer bulb at the side arm; water in at the bottom of the condenser. See boiling point determination.
Paper or thin-layer chromatography Pencil baseline above the solvent level; lid on the tank; solvent front marked immediately. See paper chromatography.
Melting point test Sample dry and packed; heated slowly near the melting point. See melting point determination.

8. Identifying substances

Skill What “good” looks like
Flame tests Clean wire loop; observe colour at the edge of a blue flame. See flame test colours.
Precipitate tests Add reagent dropwise then in excess, and state colour and what happens in excess.
Anion tests Correct acid for each test, in the correct order. See identifying ions.

9. Measuring rates and energy changes

Skill What “good” looks like
Collecting gas Gas syringe or upturned measuring cylinder; readings at regular times.
Timing a reaction Consistent end point judgement (e.g. a cross disappearing under the flask).
Measuring temperature change Insulated cup with a lid; record the maximum (or minimum) temperature. See enthalpy of neutralisation.

10. Recording data

Skill What “good” looks like
Design a results table Independent variable in the first column; units in headings, not in cells.
Consistent precision All values in a column to the same number of decimal places.
Significant figures Calculated answers to a sensible number of significant figures. See significant figures.

11. Graphs

Skill What “good” looks like
Axes and scale Independent variable on the x-axis; labels with units; scale uses more than half the grid.
Plotting Points plotted accurately as small crosses.
Line of best fit A smooth line or curve with points balanced either side; anomalies ignored and identified.
Gradients and intercepts A large triangle used for the gradient; units stated.

See graphs in chemistry.

12. Evaluating

Skill What “good” looks like
Identify variables Independent, dependent and control variables stated. See variables.
Spot anomalies Values that don’t fit the pattern are identified, with a possible reason.
Calculate percentage uncertainty Uncertainty ÷ measured value × 100. See calculating uncertainty.
Suggest specific improvements e.g. “use a burette instead of a measuring cylinder to reduce the percentage uncertainty”, not “be more careful”.

Turning the checklist into a plan

  1. List every skill rated 1 or 2.
  2. For each, read the linked guide and write the method from memory in five steps or fewer.
  3. Ask your teacher if you can repeat or watch the practical.
  4. Practise exam-style “describe” and “evaluate” questions; write the answer, then compare with the guide.
  5. Write up at least one practical in full as a lab report.

Key takeaways

  • The same core skills underpin all required practicals: safety, measurement, technique, recording and evaluation.
  • Rate yourself honestly and focus on your weakest skills.
  • Exam answers need specific equipment, specific steps and specific reasons.
  • Improvements should name a change and explain how it reduces error or uncertainty.

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